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Welcome to the Organic Chemistry Laboratory Website! Instructors:
Bruce Allison, Ph.D. Office: E-207 Mark Brandt, Ph.D. Office: FL-109 Rebecca DeVasher, Ph.D. Office: FL-103 Ross Weatherman, Ph.D. Office: FL-108 |
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| Week | Experiment
& Assignment |
Files & Handouts |
Deliverables |
| 1 (Nov. 26-30) |
Check-in, Microwave Synthesis of Tetraphenylporphyrin | Videos: Rotary Evaporator, Thin-layer Chromatography See also the lab procedure video posted on Angel |
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| 2 (Dec. 3-7) |
Column
Chromatography of
Tetraphenylporphyrin |
Videos: Column Chromatography |
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| 3 (Dec. 10-14) |
Fermentation
and distillation of molasses |
pdf: Distillation Theory Videos: Distillation |
Pair Report for Synthesis and Purification of Tetraphenylporphyrin due (see rubric and report guidelines for more instructions) |
| 4 (Dec. 17-21) |
No laboratory scheduled
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Pair Report for Fermentation and Distillation due (see rubric and report guidelines for more instructions) | |
| Christmas
Break (December 24, 2012-January 4, 2013) |
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| 5 (Jan. 7-11) |
Alkyne Coupling |
Videos: Alkyne coupling |
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| 6 (Jan. 14-18) |
NMR Spectroscopy | pdf: NMR Theory and
Practice Videos: Running the 90 MHz NMR |
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| 7 (Jan. 21-25) |
Electrophilic Aromatic Substitution, Part I | pdf: EAS Procedure Videos: EAS of Vanillin |
Pair Report for Alkyne Coupling
(including NMR spectrum analysis) due |
| 8 (Jan. 28- Feb. 1) |
Electrophilic Aromatic Substitution, Part II | |
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| 9 (Feb. 4-8) |
Lab Practicals | Core Competency Checklist |
Pair Report for Electrophilic Aromatic
Substitution due |
| 10 (Feb.11-15) |
Course Evaluation for Lab! Lab Practicals Check-out |
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