| Week |
Experiment
& Assignment
|
Files & Handouts
|
Deliverables
|
1
(Nov. 28 - Dec. 2)
|
Check-in, Resin-Based
Oxidation Chemistry
|
Oxidation Lab
Protocol
Quiz
Post-lab Report Guidelines
Recrystallization Theory
IR Spectroscopy
JACS 1976 paper
Videos: Pre-Lab Video
Recrystallization Video
Rotary Evaporation Video
Melting Point Video
|
|
2
(Dec. 5-9)
|
Gas-phase
Synthesis of Tetraphenyl porphyrin
|
Protocol
Quiz
Videos: Pre-Lab Video
TLC Video
|
|
3
(Dec. 12-16)
|
Column
Chromatography and Visible
Spectroscopy of Tetraphenylporphyrin
|
|
Pair
Report for Resin-Based
Oxidation Chemistry due (see rubric and report
guidelines for more instructions).
|
4
(Dec. 19- Jan. 6)
|
Split week
No laboratory scheduled
|
|
Pair Report for Synthesis, Purification, and Spectroscopy of
Tetraphenylporphyrin due (see rubric and
report guidelines for more instructions) |
Christmas
Break (December 21, 2011-January 3, 2012)
|
5
(Jan. 9-13) |
Metallation of Tetraphenylporphyrin
|
|
|
6
(Jan. 16-20) |
Spartan:
Conjugated Systems (Please bring your laptop to lab) |
|
Pair Report for Metallation of Tetraphenylporphyrin due
|
7
(Jan. 23-27) |
Electrophilic Aromatic Substitution, Part I |
|
Individual
Report for Spartan:
Conjugated Systems due |
8
(Jan. 30- Feb. 3)
|
Electrophilic
Aromatic Substitution, Part II |
|
|
9
(Feb. 6-10)
|
Lab Practicals |
Core Competency Checklist
|
Pair
Report for Electrophilic
Aromatic Substitution due
|
10
(Feb.13-17)
|
Course Evaluation for Lab!
Lab
Practicals
Check-out
|
|
|
