LABORATORY CHEMICAL SAFETY PROGRAM

 

ROSE-HULMAN INSTITUTE OF TECHNOLOGY

 

 

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TABLE OF CONTENTS

 

Emergency Information

 

Laboratory Safety Personnel Contacts

 

1.0 Introduction

 

·        1.1 Regulatory Basis

·        1.2 Responsibility for Implementation

o       1.2.1 Academic Departments

o       1.2.2 Faculty Members

o       1.2.3 Laboratory and Stockroom Student Worker

·        1.3 Organization and Content

 

2.0 Control Measures

 

·        2.1 Administrative Controls

o       2.1.1 Prior Approval of Hazardous Operations

o       2.1.2 Laboratory Entrance Signs

·        2.2 Engineering Controls

·        2.3 Procedural Controls

·        2.4 Personal Protective Equipment

o       2.4.1 Eye Protection

o     2.4.2 Face Protection

o     2.4.3 Hand Protection

o     2.4.4 Foot Protection

o     2.4.5 Body Protection

o     2.4.6 Respiratory Protection

 

3.0 Standard Operating Procedures

 

·        3.1 General Laboratory Safety Procedures

·        3.2 Procedures for Proper Labeling and Safe Storage of Chemicals

·        3.3 Chemical Fume Hood - Procedures for Proper and Safe Use

·        3.4 Corrosive Chemicals - Procedures for Safe Handling and Storage

·        3.5 Flammable and Combustible Liquids - Procedures for Safe Handling

·        and Storage

·        3.6 Oxidizing Agents - Procedures for Safe Handling and Storage

·        3.7 Reactive Chemicals - Procedures for Safe Handling and Storage

·        3.8 Carcinogens, Reproductive Toxins, and Acutely Toxic Chemicals -

·        Procedures for Safe Handling and Storage

·        3.9 Compressed Gases - Procedures for Safe Handling and Storage

·        3.10 Cryogenic Liquids - Procedures for Safe Handling and Storage

·        3.11 Electrical Safety Procedures

·        3.12 Glassware and Sharps - Procedures for Safe Handling and Disposal

·        3.13 Chemical Spill Response Procedures

 

4.0 Information and Training

 

·        4.1 Required Training Content

·        4.2 Training Resources

·        4.3 Training Documentation

 

5.0 Medical Consultations and Examinations

 

·        5.1 Examination Criteria

·        5.2 Information to the Physician

·        5.3 Physician's Written Opinion

·        5.4 Campus Medical Services

 

6.0 Laboratory Safety Equipment

 

·        6.1 Chemical Fume Hoods

·        6.2 Safety Showers

·        6.3 Eyewash Stations

·        6.4 Fire Extinguishers

·        6.5 Fire Blankets

·        6.6 Flammable Liquid Storage Cabinets

·        6.7 Safety Cans

·        6.8 Explosion-Proof and Laboratory-Safe Refrigeration Equipment

·        6.9 First Aid Kits

·        6.10 Chemical Spill Kits

·        6.11 Portable Safety Shields

 

 

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EMERGENCY INFORMATION

 

Major Emergencies

 

In the event of an accident in the laboratory which involves an uncontrolled fire, explosion, or a large release of a hazardous chemical:

 

·        Evacuate the building by activating the nearest fire alarm.

 

·        Call 8911 and give the details of the accident including the location, types of hazardous material involved, and whether there were any personal injuries.

 

If the accident involves serious personal injury or chemical contamination, follow the above steps as appropriate and at the same time:

 

·        Move the victim from the immediate area of the fire, explosion, or spill (if this can be done without further injury to the victim or you).

 

·        Remove any contaminated clothing from the victim and flush all areas of the body contacted by chemicals with copious amounts of water for 15 minutes.

 

Minor Emergencies

 

In the event of an accident in the laboratory which involves a minor chemical release or spill (with no personal injuries):

 

·        Follow the Chemical Spill Response Procedures - SOP 3.13.

 

·        Call 8124 for advice or assistance (8:00 a.m. - 5:00 p.m. Monday - Friday). After hours, call the Rose-Hulman Institute of Technology Security at 8911.

 

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EMERGENCY & LABORATORY SAFETY CONTACTS

 

Police, Fire Department, Ambulance                                                     9-911

Rose-Hulman Institute of Technology Security                           8911

Environmental Health and Safety Officer –Mike Howard                       8124

Cyndi Brush                                                                                         8206

David Erwin                                                                                         8476

Frank Cunning                                                                          8380

Physics                                                                                     TBD

Facilities                                                                                               TBD

 

 

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1.0 INTRODUCTION

 

The Laboratory Chemical Safety Plan is a written program for ensuring the safe use of chemicals in laboratories at Rose-Hulman Institute of Technology. It describes policies, procedures, and control measures which must be understood and observed by all individuals involved in the laboratory use of chemicals.

 

1.1 Regulatory Basis

 

The development and implementation of a Laboratory Chemical Safety Plan (or Chemical Hygiene Plan) is a central requirement of the federal rule entitled “Occupational Exposure to Hazardous Chemicals in Laboratories,” more commonly referenced as the Occupational Safety and Health  Administration (OSHA) “Lab Standard” (Appendix A contains a copy of the standard). The Lab Standard was published as a “final rule” in the January 31, 1990 issue of the Federal Register and was required to be fully implemented by January 31, 1991. Of particular importance in understanding the applicability of this standard are the definitions it contains for “hazardous chemical,” “laboratory,” “laboratory scale,” and “laboratory use of hazardous chemicals.” From a review of these definitions, it is clear that the Lab Standard applies to essentially all chemical use laboratories at Rose-Hulman Institute of Technology. For laboratories that are not covered by the Lab Standard (i.e., those that do not meet the above definitions for hazardous chemical use) or for non-laboratory uses of chemicals, safety issues are typically governed by other state and federal regulations such as OSHA's “Hazard Communication Standard.”

 

1.2 Responsibility for Implementation

 

It is the policy of Rose-Hulman Institute of Technology to support the use of chemicals and other potentially hazardous materials for purposes of research and teaching. At the same time, the Institute is committed to ensuring the safety of its students, employees, and visitors and to complying with all regulatory requirements which impact its facilities and operations. Toward this end, Rose-Hulman Institute of Technology has designated the following specific responsibilities for developing and implementing the Laboratory Chemical Safety Plan.

 

1.2.1 Academic Departments

 

The head of each academic department is responsible for the safety of all individuals working in the department's laboratories. The head fulfills this responsibility, in part, by ensuring that all departmental faculty members understand and take seriously their roles in implementing the Laboratory Chemical Safety Plan.  To facilitate this process, each head must appoint a departmental Laboratory Chemical Safety Officer (LCSO) who will coordinate and monitor the implementation of the LCSP within the department.

 

1.2.2 Faculty Members

 

Each faculty member (or principal investigator) is responsible for the safety of individuals working within his or her laboratories. Toward this end, faculty members must work with the respective departmental Laboratory Chemical Safety Officer to adapt and implement the provisions of the Laboratory Chemical Safety Plan. This includes ensuring that each individual working within the lab is provided with appropriate training on safety and regulatory requirements; that required safety equipment and personal protective devices are provided, maintained, and used; that specific standard operating procedures incorporating safety considerations are developed and observed; and that prompt action is taken to correct any unsafe acts or conditions which have been observed or reported.

 

1.2.3 Laboratory and Stockroom Student Workers

 

Each laboratory and stockroom student worker is responsible for implementing the requirements of    the Laboratory Chemical Safety Plan. This includes participating in required training, utilizing appropriate safety equipment and personal protection devices and apparel, observing standard operating procedures and informing the supervisor (i.e., principal investigator or lab supervisor)                  of any accidents or unsafe conditions.

 

1.3 Organization and Content

 

The Laboratory Chemical Safety Plan (LCSP) is intended to serve as an operational guide for the incorporation of prudent safety practices into the day-to-day use of chemicals within laboratories. It was developed and issued in a general form which should be adapted and expanded by particular departments and research groups to meet their specific needs. The LCSP was organized in a format that should enable desired information to be quickly found and readily updated. The content of the LCSP was established directly from the requirements of the Lab Standard and includes the following general types of information:

 

·        Designation of the personnel responsible for the implementation of the                    Laboratory Chemical Safety Plan.

 

·        Criteria that the employer will use to implement control measures to reduce individual exposures to chemicals. These measures include administrative controls, engineering controls, procedural controls, and the use of personal protective equipment.

 

·        Standard operating procedures (SOP’s) relevant to safety and health considerations which are to be observed for the use of hazardous chemicals in the laboratory. A number of generic SOP’s have been included in the LCSP. However, each laboratory group should develop and add specific SOP’s which are appropriate for their particular uses                                 of chemicals.

 

·        Provisions for personnel training.

 

·        Provisions for medical consultations and examinations.

 

·        Circumstances under which a laboratory procedure shall require prior                    approval before implementation.

 

·        Provisions for additional personnel protection for work with carcinogens, reproductive toxins, and chemicals with high acute toxicity.

 

·        A requirement that fume hoods and other protective equipment function properly and that measures will be taken to ensure this.

 

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2.0 CONTROL MEASURES

 

The OSHA Lab Standard requires that laboratory personnel implement appropriate control measures to ensure that chemical exposures are maintained below regulatory limits and as low as reasonably achievable. In general, control measures can be categorized as administrative controls,  engineering controls, procedural controls (i.e., standard operating procedures), or personal protection.

 

2.1 Administrative Controls

 

Administrative controls consist of various policies and requirements which are established at an administrative level (e.g., by the department head, department safety committee, or Institute Laboratory Chemical Safety Committee) to promote safety in the laboratory.  They may include:

 

·        Ensuring that all laboratory personnel have been provided with adequate training to enable them to conduct their duties safely (see Section 4.0 Information and Training).

 

·        Requiring prior approval and additional control measures for certain                particularly hazardous operations or activities.

 

·        Restricting access to areas in which particularly hazardous chemicals                                  are used.

 

·        Posting appropriate signs to identify specific hazards within an area.

 

·        Requiring that various standard practices for chemical safety and good           housekeeping be observed at all times in the laboratory.

 

2.1.1 Prior Approval of Hazardous Operations

 

The OSHA Lab Standard requires that activities which involve certain particularly hazardous chemicals be reviewed and approved in advance by an appropriate individual or group. Depending upon the specific department, this approving entity could be a department safety committee, the Laboratory Chemical Safety Officer, or the department head. At the time of approval, any additional required control measures for the project should be specified. Examples of the types of operations which should receive prior approval are those involving the use of select carcinogens,   reproductive toxins, acutely toxic chemicals, highly reactive or shock sensitive chemicals, or highly corrosive or oxidizing chemicals. In addition, any operation that produces unknown but       potentially hazardous results should receive prior approval.

 

2.1.2 Laboratory Entrance Signs

 

The entrance to each laboratory in which chemicals are used or stored shall be posted with the names and phone numbers of the principal investigator (or lab supervisor) and any other designated personnel who can be contacted in the event of an emergency. In addition, laboratory entrance postings should indicate the presence of certain specific hazards.

 

2.2 Engineering Controls

 

Engineering controls consist of various measures for reducing a hazard at its source or for separating personnel from the hazard. In the laboratory, examples of engineering controls include the substitution of less hazardous chemicals in an operation, isolating a particular chemical operation, enclosing a potentially explosive reaction, or utilizing local exhaust such as a fume hood for an operation which produces airborne chemicals (see Section 6.1 Chemical Fume Hoods). Because engineering controls function to reduce or eliminate a hazard at its source before it is created, they should be fully considered and utilized whenever possible as the first step in chemical hazard control within the laboratory.

 

2.3 Procedural Controls

 

Procedural controls (or work practice controls) are typically in the form of standard operating procedures (SOP’s) which define the manner in which certain types of chemicals are to be handled, or the manner in which specific operations involving chemicals are to be conducted, in order to minimize hazards. Section 3.0 of this Plan contains a number of SOP’s which are generally applicable to all laboratories. It is the responsibility of personnel in each laboratory, however, to develop (and incorporate into the LCSP) specific SOP’s which reflect the operations and experimental protocols performed in their laboratory.

 

2.4 Personal Protective Equipment

 

For many laboratory operations, the risk of chemical exposure cannot be totally eliminated through the use of engineering and procedural control measures. For this reason, it is necessary to supplement such measures with the use of personal protective equipment and apparel (PPE). Because PPE functions as a barrier between the laboratory worker and the chemical hazard, rather than by actually reducing or eliminating the hazard, its use should always be in addition to (and never as a substitute for) appropriate engineering and procedural controls. It is the responsibility of the principal investigator (or supervisor) of the laboratory to ensure that appropriate personal protective equipment is provided to, and used by, all laboratory personnel. Such equipment should be adequate to ensure personnel are protected from chemical exposure to the eyes, skin, and respiratory tract.

 

 

 

2.4.1 Eye Protection